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Ultrasonic energy input influence on the production of sub-micron o/w emulsions containing whey protein and common stabilizers

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dc.contributor.author Kaltsa, O en
dc.contributor.author Michon, C en
dc.contributor.author Yanniotis, S en
dc.contributor.author Mandala, I en
dc.date.accessioned 2014-06-06T06:52:54Z
dc.date.available 2014-06-06T06:52:54Z
dc.date.issued 2013 en
dc.identifier.issn 13504177 en
dc.identifier.uri http://dx.doi.org/10.1016/j.ultsonch.2012.11.011 en
dc.identifier.uri http://62.217.125.90/xmlui/handle/123456789/6243
dc.subject Emulsion en
dc.subject Gums en
dc.subject Ultrasound en
dc.subject Whey en
dc.subject.other Depletion flocculation en
dc.subject.other Dispersed phase en
dc.subject.other Droplet sizes en
dc.subject.other Emulsion formation en
dc.subject.other Energy inputs en
dc.subject.other Gums en
dc.subject.other High-energy input en
dc.subject.other O/W emulsions en
dc.subject.other Oil droplets en
dc.subject.other Oil formation en
dc.subject.other Olive oil en
dc.subject.other Optical micrographs en
dc.subject.other Storage periods en
dc.subject.other Structural modifications en
dc.subject.other Submicron en
dc.subject.other Ultra-sonication en
dc.subject.other Ultrasonic emulsification en
dc.subject.other Ultrasonic energy en
dc.subject.other Viscosity reduction en
dc.subject.other Viscosity value en
dc.subject.other Whey en
dc.subject.other Whey proteins en
dc.subject.other Drops en
dc.subject.other Emulsions en
dc.subject.other Flocculation en
dc.subject.other Particle size analysis en
dc.subject.other Proteins en
dc.subject.other Stability en
dc.subject.other Turbidity en
dc.subject.other Ultrasonic applications en
dc.subject.other Ultrasonics en
dc.subject.other Vegetable oils en
dc.subject.other Emulsification en
dc.subject.other milk protein en
dc.subject.other olive oil en
dc.subject.other article en
dc.subject.other concentration (parameters) en
dc.subject.other crystallization en
dc.subject.other differential scanning calorimetry en
dc.subject.other emulsion en
dc.subject.other enthalpy en
dc.subject.other flocculation en
dc.subject.other high intensity ultrasonication en
dc.subject.other hydrocolloid en
dc.subject.other microphotography en
dc.subject.other particle size en
dc.subject.other pH en
dc.subject.other priority journal en
dc.subject.other procedures en
dc.subject.other turbidity en
dc.subject.other ultrasound en
dc.subject.other viscosity en
dc.subject.other Emulsifying Agents en
dc.subject.other Emulsions en
dc.subject.other Food Industry en
dc.subject.other Food Storage en
dc.subject.other Milk Proteins en
dc.subject.other Particle Size en
dc.subject.other Plant Oils en
dc.subject.other Sonication en
dc.subject.other Viscosity en
dc.subject.other Water en
dc.title Ultrasonic energy input influence on the production of sub-micron o/w emulsions containing whey protein and common stabilizers en
heal.type journalArticle en
heal.identifier.primary 10.1016/j.ultsonch.2012.11.011 en
heal.publicationDate 2013 en
heal.abstract Ultrasonication may be a cost-effective emulsion formation technique, but its impact on emulsion final structure and droplet size needs to be further investigated. Olive oil emulsions (20 wt%) were formulated (pH ∼ 7) using whey protein (3 wt%), three kinds of hydrocolloids (0.1-0.5 wt%) and two different emulsification energy inputs (single- and two-stage, methods A and B, respectively). Formula and energy input effects on emulsion performance are discussed. Emulsions stability was evaluated over a 10-day storage period at 5 °C recording the turbidity profiles of the emulsions. Optical micrographs, droplet size and viscosity values were also obtained. A differential scanning calorimetric (DSC) multiple cool-heat cyclic method (40 to -40 °C) was performed to examine stability via crystallization phenomena of the dispersed phase. Ultrasonication energy input duplication from 11 kJ to 25 kJ (method B) resulted in stable emulsions production (reduction of back scattering values, dBS ∼ 1% after 10 days of storage) at 0.5 wt% concentration of any of the stabilizers used. At lower gum amount samples became unstable due to depletion flocculation phenomena, regardless of emulsification energy input used. High energy input during ultrasonic emulsification also resulted in sub-micron oil-droplets emulsions (D50 = 0.615 μm compared to D50 = 1.3 μm using method A) with narrower particle size distribution and in viscosity reduction. DSC experiments revealed no presence of bulk oil formation, suggesting stability for XG 0.5 wt% emulsions prepared by both methods. Reduced enthalpy values found when method B was applied suggesting structural modifications produced by extensive ultrasonication. Change of ultrasonication conditions results in significant changes of oil droplet size and stability of the produced emulsions. © 2012 Elsevier B.V. All rights reserved. en
heal.journalName Ultrasonics Sonochemistry en
dc.identifier.issue 3 en
dc.identifier.volume 20 en
dc.identifier.doi 10.1016/j.ultsonch.2012.11.011 en
dc.identifier.spage 881 en
dc.identifier.epage 891 en


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