| dc.contributor.author |
Anagnostopoulos, CJ |
en |
| dc.contributor.author |
Aplada Sarli, P |
en |
| dc.contributor.author |
Miliadis, GE |
en |
| dc.contributor.author |
Haroutounian, CA |
en |
| dc.date.accessioned |
2014-06-06T06:49:51Z |
|
| dc.date.available |
2014-06-06T06:49:51Z |
|
| dc.date.issued |
2010 |
en |
| dc.identifier.issn |
17913691 |
en |
| dc.identifier.uri |
http://62.217.125.90/xmlui/handle/123456789/4837 |
|
| dc.relation.uri |
http://www.scopus.com/inward/record.url?eid=2-s2.0-77956719898&partnerID=40&md5=da3cb84d6ec68ccbd297f4ee78ffa61c |
en |
| dc.subject |
GC-ECD |
en |
| dc.subject |
GC-NPD |
en |
| dc.subject |
Linearity |
en |
| dc.subject |
Precision |
en |
| dc.subject |
Trueness |
en |
| dc.subject |
Validation |
en |
| dc.title |
Validation of the QuEChERS method for the determination of 25 priority pesticide residues in cereal-based baby foods by gas chromatography with electron capture and nitrogen phosphorous detection |
en |
| heal.type |
journalArticle |
en |
| heal.publicationDate |
2010 |
en |
| heal.abstract |
A multiresidue method for the simultaneous analysis of 25 pesticides and metabolites included in Commission Directives 2006/141/EC and 2006/125/EC for baby food was validated in cerealbased baby foods. The extraction procedure was based on the QuEChERS method and the determination was performed by gas chromatography combined with electron capture detector (ECD) and nitrogen phosphorus detector (NPD). The analytical performance was demonstrated by the analysis of extracts of spiked samples at two concentration levels, 3 and 30 μg/kg, for each analyte. Good sensitivity and selectivity of the method were obtained with limits of quantification at 3 μg/kg in all cases. All pesticides and metabolites, with the exception of omethoate, gave recovery values ranging from 79.2 to 124.6% with relative standard deviations less than 28% at both spiking levels for most analytes. © Benaki Phytopathological Institute. |
en |
| heal.journalName |
Hellenic Plant Protection Journal |
en |
| dc.identifier.issue |
2 |
en |
| dc.identifier.volume |
3 |
en |
| dc.identifier.spage |
71 |
en |
| dc.identifier.epage |
80 |
en |