| dc.contributor.author |
Kasiotis, KM |
en |
| dc.contributor.author |
Souki, H |
en |
| dc.contributor.author |
Tsakirakis, AN |
en |
| dc.contributor.author |
Carageorgiou, H |
en |
| dc.contributor.author |
Theotokatos, SA |
en |
| dc.contributor.author |
Haroutounian, SA |
en |
| dc.contributor.author |
Machera, K |
en |
| dc.date.accessioned |
2014-06-06T06:48:31Z |
|
| dc.date.available |
2014-06-06T06:48:31Z |
|
| dc.date.issued |
2008 |
en |
| dc.identifier.issn |
14220067 |
en |
| dc.identifier.uri |
http://dx.doi.org/10.3390/ijms9050906 |
en |
| dc.identifier.uri |
http://62.217.125.90/xmlui/handle/123456789/4171 |
|
| dc.subject |
Fenthion |
en |
| dc.subject |
GC/MS |
en |
| dc.subject |
Headspace |
en |
| dc.subject |
Insecticide residue |
en |
| dc.subject |
Metabolites |
en |
| dc.subject |
Olive |
en |
| dc.subject |
SPME |
en |
| dc.subject.other |
fenoxon |
en |
| dc.subject.other |
fenthion |
en |
| dc.subject.other |
insecticide |
en |
| dc.subject.other |
polyacrylic acid |
en |
| dc.subject.other |
sulfoxide |
en |
| dc.subject.other |
analytic method |
en |
| dc.subject.other |
article |
en |
| dc.subject.other |
gas chromatography |
en |
| dc.subject.other |
human |
en |
| dc.subject.other |
metabolite |
en |
| dc.subject.other |
quantitative analysis |
en |
| dc.subject.other |
serum |
en |
| dc.subject.other |
solid phase microextraction |
en |
| dc.title |
Headspace solid phase micro extraction gas chromatographic determination of fenthion in human serum |
en |
| heal.type |
journalArticle |
en |
| heal.identifier.primary |
10.3390/ijms9050906 |
en |
| heal.publicationDate |
2008 |
en |
| heal.abstract |
A simple and effective analytical procedure was developed for the determination of fenthion residues in human serum samples. The sample treatment was performed using the headspace solid-phase micro extraction with polyacrylate fiber, which has the advantage to require low amount of serum (1 mL) without tedious pre-treatment. The quantification of fenthion was carried out by gas chromatography-mass spectrometry and the recoveries ranged from 79 to 104% at two spiking levels for 6 replicates. Detection and quantification limits were calculated as 1.51 and 4.54 ng/mL of serum respectively. Two fenthion metabolites - fenoxon and fenthion-sulfoxide - were also identified. © 2008 by the authors. |
en |
| heal.journalName |
International Journal of Molecular Sciences |
en |
| dc.identifier.issue |
5 |
en |
| dc.identifier.volume |
9 |
en |
| dc.identifier.doi |
10.3390/ijms9050906 |
en |
| dc.identifier.spage |
906 |
en |
| dc.identifier.epage |
913 |
en |